Analytical TEM Observation of the Flame-Ablated Surface of Borosilicate-Glass Vials.
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| Title: | Analytical TEM Observation of the Flame-Ablated Surface of Borosilicate-Glass Vials. |
|---|---|
| Authors: | Mikamoto, K.1 (AUTHOR) mikamotokotono@keio.jp, Takeuchi, M.2 (AUTHOR), Shirakura, A.1 (AUTHOR), Suzuki, T.1 (AUTHOR) |
| Source: | Glass Physics & Chemistry. Mar2021, Vol. 47 Issue 2, p91-96. 6p. |
| Subjects: | Diamond-like carbon, Glass coatings, Borosilicates, Vials, Transmission electron microscopy, X-ray spectroscopy, Freeze-drying, Surface coatings |
| Abstract: | We investigated the effects of the flame-ablation treatment on the inner surface of borosilicate glass vials and the adhesion of fluorinated diamond-like carbon coating to glass vials. Transmission electron microscopy with energy-dispersive X-ray spectroscopy analysis show that the flame-ablation treatment removed the less durable layers that contained sodium borate, which might cause elution and delamination in an aqueous solution, and formed a flat surface. The outermost surface of the flame-ablated inner wall of the vials formed a microcrystal layer containing Na and K. In addition, the flame-ablation treatment improved the adhesion of the coating to the glass vials. The EDX maps show that F derived from the F-DLC coating and Na and K derived from the glass were mixed and formed an interface layer between the F-DLC coating and the glass vial. This result indicates that the flame-ablation treatment is a promising method to improve the adhesion of the coating to borosilicate glass vials. [ABSTRACT FROM AUTHOR] |
| Copyright of Glass Physics & Chemistry is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.) | |
| Database: | Engineering Source |
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| Items | – Name: Title Label: Title Group: Ti Data: Analytical TEM Observation of the Flame-Ablated Surface of Borosilicate-Glass Vials. – Name: Author Label: Authors Group: Au Data: <searchLink fieldCode="AR" term="%22Mikamoto%2C+K%2E%22">Mikamoto, K.</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> mikamotokotono@keio.jp</i><br /><searchLink fieldCode="AR" term="%22Takeuchi%2C+M%2E%22">Takeuchi, M.</searchLink><relatesTo>2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Shirakura%2C+A%2E%22">Shirakura, A.</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Suzuki%2C+T%2E%22">Suzuki, T.</searchLink><relatesTo>1</relatesTo> (AUTHOR) – Name: TitleSource Label: Source Group: Src Data: <searchLink fieldCode="JN" term="%22Glass+Physics+%26+Chemistry%22">Glass Physics & Chemistry</searchLink>. Mar2021, Vol. 47 Issue 2, p91-96. 6p. – Name: Subject Label: Subjects Group: Su Data: <searchLink fieldCode="DE" term="%22Diamond-like+carbon%22">Diamond-like carbon</searchLink><br /><searchLink fieldCode="DE" term="%22Glass+coatings%22">Glass coatings</searchLink><br /><searchLink fieldCode="DE" term="%22Borosilicates%22">Borosilicates</searchLink><br /><searchLink fieldCode="DE" term="%22Vials%22">Vials</searchLink><br /><searchLink fieldCode="DE" term="%22Transmission+electron+microscopy%22">Transmission electron microscopy</searchLink><br /><searchLink fieldCode="DE" term="%22X-ray+spectroscopy%22">X-ray spectroscopy</searchLink><br /><searchLink fieldCode="DE" term="%22Freeze-drying%22">Freeze-drying</searchLink><br /><searchLink fieldCode="DE" term="%22Surface+coatings%22">Surface coatings</searchLink> – Name: Abstract Label: Abstract Group: Ab Data: We investigated the effects of the flame-ablation treatment on the inner surface of borosilicate glass vials and the adhesion of fluorinated diamond-like carbon coating to glass vials. Transmission electron microscopy with energy-dispersive X-ray spectroscopy analysis show that the flame-ablation treatment removed the less durable layers that contained sodium borate, which might cause elution and delamination in an aqueous solution, and formed a flat surface. The outermost surface of the flame-ablated inner wall of the vials formed a microcrystal layer containing Na and K. In addition, the flame-ablation treatment improved the adhesion of the coating to the glass vials. The EDX maps show that F derived from the F-DLC coating and Na and K derived from the glass were mixed and formed an interface layer between the F-DLC coating and the glass vial. This result indicates that the flame-ablation treatment is a promising method to improve the adhesion of the coating to borosilicate glass vials. [ABSTRACT FROM AUTHOR] – Name: AbstractSuppliedCopyright Label: Group: Ab Data: <i>Copyright of Glass Physics & Chemistry is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.) |
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| RecordInfo | BibRecord: BibEntity: Identifiers: – Type: doi Value: 10.1134/S1087659621020097 Languages: – Code: eng Text: English PhysicalDescription: Pagination: PageCount: 6 StartPage: 91 Subjects: – SubjectFull: Diamond-like carbon Type: general – SubjectFull: Glass coatings Type: general – SubjectFull: Borosilicates Type: general – SubjectFull: Vials Type: general – SubjectFull: Transmission electron microscopy Type: general – SubjectFull: X-ray spectroscopy Type: general – SubjectFull: Freeze-drying Type: general – SubjectFull: Surface coatings Type: general Titles: – TitleFull: Analytical TEM Observation of the Flame-Ablated Surface of Borosilicate-Glass Vials. Type: main BibRelationships: HasContributorRelationships: – PersonEntity: Name: NameFull: Mikamoto, K. – PersonEntity: Name: NameFull: Takeuchi, M. – PersonEntity: Name: NameFull: Shirakura, A. – PersonEntity: Name: NameFull: Suzuki, T. IsPartOfRelationships: – BibEntity: Dates: – D: 01 M: 03 Text: Mar2021 Type: published Y: 2021 Identifiers: – Type: issn-print Value: 10876596 Numbering: – Type: volume Value: 47 – Type: issue Value: 2 Titles: – TitleFull: Glass Physics & Chemistry Type: main |
| ResultId | 1 |
