Optimizing Thermomechanical Processing for Producing Bulk Fine-Grained Aluminum Alloy with Thermal Stability.

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Title: Optimizing Thermomechanical Processing for Producing Bulk Fine-Grained Aluminum Alloy with Thermal Stability.
Authors: Punyafu, Jesada1,2 (AUTHOR), Domrong, Chonlada1,2 (AUTHOR), Patakham, Ussadawut3 (AUTHOR), Murayama, Mitsuhiro2,4 (AUTHOR), Banjongprasert, Chaiyasit1,5 (AUTHOR) chaiyasit.b@cmu.ac.th
Source: Materials (1996-1944). Sep2025, Vol. 18 Issue 17, p4180. 7p.
Subjects: Thermal stability, Thermomechanical treatment, Material plasticity, Nanostructured materials, Aluminum alloys, Electron backscattering, Transmission electron microscopy
Abstract: This study investigates the thermal stability of fine-grained structures achieved through different severe plastic deformation (SPD) and heat treatment paths. Bulk fine-grained Al-0.1Sc-0.1Zr (wt%) alloy was produced via equal channel angular pressing (ECAP) using routes Bc or C, with aging before or after the ECAP. Electron back-scattered diffraction (EBSD) and transmission electron microscopy (TEM) analyses demonstrate excellent thermal stability of all four specimens. They maintain mean grain sizes below 5 μm after a 10 h thermal test at 450 °C, attributed to the presence of nano Al3(Sc,Zr) precipitates within the microstructures. Route Bc in the ECAP method forms more stable high-angle grain boundaries (HAGBs) than route C. Whether aging occurs before or after the ECAP, similar microstructural changes are observed after thermal testing, allowing fine-tuning of the microstructure depending on the application or subsequent processes. [ABSTRACT FROM AUTHOR]
Copyright of Materials (1996-1944) is the property of MDPI and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Data: Optimizing Thermomechanical Processing for Producing Bulk Fine-Grained Aluminum Alloy with Thermal Stability.
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  Data: <searchLink fieldCode="JN" term="%22Materials+%281996-1944%29%22">Materials (1996-1944)</searchLink>. Sep2025, Vol. 18 Issue 17, p4180. 7p.
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  Data: <searchLink fieldCode="DE" term="%22Thermal+stability%22">Thermal stability</searchLink><br /><searchLink fieldCode="DE" term="%22Thermomechanical+treatment%22">Thermomechanical treatment</searchLink><br /><searchLink fieldCode="DE" term="%22Material+plasticity%22">Material plasticity</searchLink><br /><searchLink fieldCode="DE" term="%22Nanostructured+materials%22">Nanostructured materials</searchLink><br /><searchLink fieldCode="DE" term="%22Aluminum+alloys%22">Aluminum alloys</searchLink><br /><searchLink fieldCode="DE" term="%22Electron+backscattering%22">Electron backscattering</searchLink><br /><searchLink fieldCode="DE" term="%22Transmission+electron+microscopy%22">Transmission electron microscopy</searchLink>
– Name: Abstract
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  Data: This study investigates the thermal stability of fine-grained structures achieved through different severe plastic deformation (SPD) and heat treatment paths. Bulk fine-grained Al-0.1Sc-0.1Zr (wt%) alloy was produced via equal channel angular pressing (ECAP) using routes Bc or C, with aging before or after the ECAP. Electron back-scattered diffraction (EBSD) and transmission electron microscopy (TEM) analyses demonstrate excellent thermal stability of all four specimens. They maintain mean grain sizes below 5 μm after a 10 h thermal test at 450 °C, attributed to the presence of nano Al3(Sc,Zr) precipitates within the microstructures. Route Bc in the ECAP method forms more stable high-angle grain boundaries (HAGBs) than route C. Whether aging occurs before or after the ECAP, similar microstructural changes are observed after thermal testing, allowing fine-tuning of the microstructure depending on the application or subsequent processes. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Materials (1996-1944) is the property of MDPI and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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RecordInfo BibRecord:
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      – Type: doi
        Value: 10.3390/ma18174180
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      – Code: eng
        Text: English
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        PageCount: 7
        StartPage: 4180
    Subjects:
      – SubjectFull: Thermal stability
        Type: general
      – SubjectFull: Thermomechanical treatment
        Type: general
      – SubjectFull: Material plasticity
        Type: general
      – SubjectFull: Nanostructured materials
        Type: general
      – SubjectFull: Aluminum alloys
        Type: general
      – SubjectFull: Electron backscattering
        Type: general
      – SubjectFull: Transmission electron microscopy
        Type: general
    Titles:
      – TitleFull: Optimizing Thermomechanical Processing for Producing Bulk Fine-Grained Aluminum Alloy with Thermal Stability.
        Type: main
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          Name:
            NameFull: Punyafu, Jesada
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            NameFull: Domrong, Chonlada
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            NameFull: Patakham, Ussadawut
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            NameFull: Murayama, Mitsuhiro
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            NameFull: Banjongprasert, Chaiyasit
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            – D: 01
              M: 09
              Text: Sep2025
              Type: published
              Y: 2025
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              Value: 18
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              Value: 17
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            – TitleFull: Materials (1996-1944)
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