Tailoring the microstructure homogeneity to improve the mechanical property of Ti-6Al-4V alloy through heavily warm rolling acicular martensitic microstructure.

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Title: Tailoring the microstructure homogeneity to improve the mechanical property of Ti-6Al-4V alloy through heavily warm rolling acicular martensitic microstructure.
Authors: Wu, Xiaofeng1 (AUTHOR), Fu, Liming1 (AUTHOR) lmfu@sjtu.edu.cn, Ma, Shuo1 (AUTHOR), Wen, Mao1 (AUTHOR), Shan, Aidang1 (AUTHOR) adshan@sjtu.edu.cn
Source: Journal of Materials Science. Feb2026, Vol. 61 Issue 5, p3340-3363. 24p.
Subjects: Microstructure, Martensite, Titanium alloys, Cold rolling, Mechanical behavior of materials, Recrystallization (Metallurgy), Hot working, Deformations (Mechanics)
Abstract: Micro-textured regions (MTRs), which are formed by thermomechanical processing of titanium alloys with α + β lamellar structure, induce incompatible deformation and result in early crack initiation during plastic deformation. In this study, we developed an innovative thermomechanical processing routine that eliminates the formation of band-like MTRs in Ti-6Al-4V alloy. The first step of this routine is solution treatment at 1050 °C for 20 min followed by ice water quenching, to obtain an initial microstructure of full acicular α' martensite. As a comparison, a sample with typical α + β lamellar structure was fabricated by solution treatment at 1050 °C for 20 min followed furnace cooling. Thereafter, both the two samples were processed with a heavy warm rolling procedure at 700 °C and an annealing treatment at 700 °C for one hours. Microstructure characterization showed that after heavy warm rolling and subsequent annealing at 700 °C, acicular α' martensitic transform into homogeneous and random fine equiaxed grains. This is in contrast with the annealed α + β lamellar structure that a large number of band-like MTRs are formed. Mechanical properties of the sample with annealed martensite are thus significantly improved due to the elimination of MTRs. The strength reaches 1100 MPa, and the total elongation is approximately 14.3%, nearly twice that of the annealed α + β lamellar structure. [ABSTRACT FROM AUTHOR]
Copyright of Journal of Materials Science is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Data: Tailoring the microstructure homogeneity to improve the mechanical property of Ti-6Al-4V alloy through heavily warm rolling acicular martensitic microstructure.
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  Data: <searchLink fieldCode="AR" term="%22Wu%2C+Xiaofeng%22">Wu, Xiaofeng</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Fu%2C+Liming%22">Fu, Liming</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> lmfu@sjtu.edu.cn</i><br /><searchLink fieldCode="AR" term="%22Ma%2C+Shuo%22">Ma, Shuo</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Wen%2C+Mao%22">Wen, Mao</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Shan%2C+Aidang%22">Shan, Aidang</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> adshan@sjtu.edu.cn</i>
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  Data: <searchLink fieldCode="DE" term="%22Microstructure%22">Microstructure</searchLink><br /><searchLink fieldCode="DE" term="%22Martensite%22">Martensite</searchLink><br /><searchLink fieldCode="DE" term="%22Titanium+alloys%22">Titanium alloys</searchLink><br /><searchLink fieldCode="DE" term="%22Cold+rolling%22">Cold rolling</searchLink><br /><searchLink fieldCode="DE" term="%22Mechanical+behavior+of+materials%22">Mechanical behavior of materials</searchLink><br /><searchLink fieldCode="DE" term="%22Recrystallization+%28Metallurgy%29%22">Recrystallization (Metallurgy)</searchLink><br /><searchLink fieldCode="DE" term="%22Hot+working%22">Hot working</searchLink><br /><searchLink fieldCode="DE" term="%22Deformations+%28Mechanics%29%22">Deformations (Mechanics)</searchLink>
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  Label: Abstract
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  Data: Micro-textured regions (MTRs), which are formed by thermomechanical processing of titanium alloys with α + β lamellar structure, induce incompatible deformation and result in early crack initiation during plastic deformation. In this study, we developed an innovative thermomechanical processing routine that eliminates the formation of band-like MTRs in Ti-6Al-4V alloy. The first step of this routine is solution treatment at 1050 °C for 20 min followed by ice water quenching, to obtain an initial microstructure of full acicular α' martensite. As a comparison, a sample with typical α + β lamellar structure was fabricated by solution treatment at 1050 °C for 20 min followed furnace cooling. Thereafter, both the two samples were processed with a heavy warm rolling procedure at 700 °C and an annealing treatment at 700 °C for one hours. Microstructure characterization showed that after heavy warm rolling and subsequent annealing at 700 °C, acicular α' martensitic transform into homogeneous and random fine equiaxed grains. This is in contrast with the annealed α + β lamellar structure that a large number of band-like MTRs are formed. Mechanical properties of the sample with annealed martensite are thus significantly improved due to the elimination of MTRs. The strength reaches 1100 MPa, and the total elongation is approximately 14.3%, nearly twice that of the annealed α + β lamellar structure. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Journal of Materials Science is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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RecordInfo BibRecord:
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      – Type: doi
        Value: 10.1007/s10853-025-11621-y
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      – Code: eng
        Text: English
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        PageCount: 24
        StartPage: 3340
    Subjects:
      – SubjectFull: Microstructure
        Type: general
      – SubjectFull: Martensite
        Type: general
      – SubjectFull: Titanium alloys
        Type: general
      – SubjectFull: Cold rolling
        Type: general
      – SubjectFull: Mechanical behavior of materials
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      – SubjectFull: Recrystallization (Metallurgy)
        Type: general
      – SubjectFull: Hot working
        Type: general
      – SubjectFull: Deformations (Mechanics)
        Type: general
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      – TitleFull: Tailoring the microstructure homogeneity to improve the mechanical property of Ti-6Al-4V alloy through heavily warm rolling acicular martensitic microstructure.
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            NameFull: Wu, Xiaofeng
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            NameFull: Fu, Liming
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            NameFull: Ma, Shuo
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            NameFull: Wen, Mao
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            – D: 01
              M: 02
              Text: Feb2026
              Type: published
              Y: 2026
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              Value: 61
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