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MXene (Ti3C2) an Effective Adsorbent for Micro Solid Phase Extraction of Trace Lead from Water and Tobacco Samples.

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Title: MXene (Ti3C2) an Effective Adsorbent for Micro Solid Phase Extraction of Trace Lead from Water and Tobacco Samples.
Authors: Kori, Abdul Hameed1,2 (AUTHOR) abdulhameed@scholars.usindh.edu.pk, Uzcan, Furkan1,3 (AUTHOR) furkanuzcan@erciyes.edu.tr, Soylak, Mustafa1,3,4 (AUTHOR) soylak@erciyes.edu.tr
Source: Water, Air & Soil Pollution. Feb2026, Vol. 237 Issue 3, p1-12. 12p.
Subject Terms: *Solid phase extraction, *Water sampling, *Tobacco products, *Titanium carbide, *Sorbents, *Analytical chemistry, *Analytical chemistry techniques, *Nanostructured materials
Abstract: A micro-solid-phase extraction (μSPE) method has been proposed for the separation-preconcentration of lead on MXene (Ti3C2), prior to its high-resolution continuum source flame atomic absorption spectrometry (HR-CS-FAAS) detection. MXene was produced and characterized with a variety of methods, including Fourier-transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), scanning transmission electron microscopy (STEM), and X-ray diffraction. To optimize a variety of factors, including pH, eluent type, MXene quantity, and contact duration "one-factor-at-a-time" method was used. The MX-μSPE process included dispersing the MXene in the sample solution and then separating it from the matrix. The improved technique has limit of detection (LOD) of 0.5 µg L−1, and a preconcentration factor of 20. Two different certified reference materials were used to verify the accuracy of the proposed procedure. The procedure was applied to determination of lead contents of water and tobacco samples. [ABSTRACT FROM AUTHOR]
Database: Energy & Power Source
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Header DbId: enr
DbLabel: Energy & Power Source
An: 190506580
AccessLevel: 6
PubType: Academic Journal
PubTypeId: academicJournal
PreciseRelevancyScore: 0
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  Label: Title
  Group: Ti
  Data: MXene (Ti<subscript>3</subscript>C<subscript>2</subscript>) an Effective Adsorbent for Micro Solid Phase Extraction of Trace Lead from Water and Tobacco Samples.
– Name: Author
  Label: Authors
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  Data: <searchLink fieldCode="AR" term="%22Kori%2C+Abdul+Hameed%22">Kori, Abdul Hameed</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<i> abdulhameed@scholars.usindh.edu.pk</i><br /><searchLink fieldCode="AR" term="%22Uzcan%2C+Furkan%22">Uzcan, Furkan</searchLink><relatesTo>1,3</relatesTo> (AUTHOR)<i> furkanuzcan@erciyes.edu.tr</i><br /><searchLink fieldCode="AR" term="%22Soylak%2C+Mustafa%22">Soylak, Mustafa</searchLink><relatesTo>1,3,4</relatesTo> (AUTHOR)<i> soylak@erciyes.edu.tr</i>
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  Data: <searchLink fieldCode="JN" term="%22Water%2C+Air+%26+Soil+Pollution%22">Water, Air & Soil Pollution</searchLink>. Feb2026, Vol. 237 Issue 3, p1-12. 12p.
– Name: Subject
  Label: Subject Terms
  Group: Su
  Data: *<searchLink fieldCode="DE" term="%22Solid+phase+extraction%22">Solid phase extraction</searchLink><br />*<searchLink fieldCode="DE" term="%22Water+sampling%22">Water sampling</searchLink><br />*<searchLink fieldCode="DE" term="%22Tobacco+products%22">Tobacco products</searchLink><br />*<searchLink fieldCode="DE" term="%22Titanium+carbide%22">Titanium carbide</searchLink><br />*<searchLink fieldCode="DE" term="%22Sorbents%22">Sorbents</searchLink><br />*<searchLink fieldCode="DE" term="%22Analytical+chemistry%22">Analytical chemistry</searchLink><br />*<searchLink fieldCode="DE" term="%22Analytical+chemistry+techniques%22">Analytical chemistry techniques</searchLink><br />*<searchLink fieldCode="DE" term="%22Nanostructured+materials%22">Nanostructured materials</searchLink>
– Name: Abstract
  Label: Abstract
  Group: Ab
  Data: A micro-solid-phase extraction (μSPE) method has been proposed for the separation-preconcentration of lead on MXene (Ti3C2), prior to its high-resolution continuum source flame atomic absorption spectrometry (HR-CS-FAAS) detection. MXene was produced and characterized with a variety of methods, including Fourier-transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), scanning transmission electron microscopy (STEM), and X-ray diffraction. To optimize a variety of factors, including pH, eluent type, MXene quantity, and contact duration "one-factor-at-a-time" method was used. The MX-μSPE process included dispersing the MXene in the sample solution and then separating it from the matrix. The improved technique has limit of detection (LOD) of 0.5 µg L−1, and a preconcentration factor of 20. Two different certified reference materials were used to verify the accuracy of the proposed procedure. The procedure was applied to determination of lead contents of water and tobacco samples. [ABSTRACT FROM AUTHOR]
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RecordInfo BibRecord:
  BibEntity:
    Identifiers:
      – Type: doi
        Value: 10.1007/s11270-025-08888-x
    Languages:
      – Code: eng
        Text: English
    PhysicalDescription:
      Pagination:
        PageCount: 12
        StartPage: 1
    Subjects:
      – SubjectFull: Solid phase extraction
        Type: general
      – SubjectFull: Water sampling
        Type: general
      – SubjectFull: Tobacco products
        Type: general
      – SubjectFull: Titanium carbide
        Type: general
      – SubjectFull: Sorbents
        Type: general
      – SubjectFull: Analytical chemistry
        Type: general
      – SubjectFull: Analytical chemistry techniques
        Type: general
      – SubjectFull: Nanostructured materials
        Type: general
    Titles:
      – TitleFull: MXene (Ti3C2) an Effective Adsorbent for Micro Solid Phase Extraction of Trace Lead from Water and Tobacco Samples.
        Type: main
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          Name:
            NameFull: Kori, Abdul Hameed
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            NameFull: Uzcan, Furkan
      – PersonEntity:
          Name:
            NameFull: Soylak, Mustafa
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          Dates:
            – D: 01
              M: 02
              Text: Feb2026
              Type: published
              Y: 2026
          Identifiers:
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              Value: 00496979
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              Value: 237
            – Type: issue
              Value: 3
          Titles:
            – TitleFull: Water, Air & Soil Pollution
              Type: main
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