Exploring Electrochromics: A Series of Eye-Catching Experiments to Introduce Students to Multidisciplinary Research

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Bibliographic Details
Title: Exploring Electrochromics: A Series of Eye-Catching Experiments to Introduce Students to Multidisciplinary Research
Language: English
Authors: Small, Leo J., Wolf, Steven, Spoerke, Erik D.
Source: Journal of Chemical Education. Dec 2014 91(12):2099-2104.
Availability: Division of Chemical Education, Inc and ACS Publications Division of the American Chemical Society. 1155 Sixteenth Street NW, Washington, DC 20036. Tel: 800-227-5558; Tel: 202-872-4600; e-mail: eic@jce.acs.org; Web site: http://pubs.acs.org/jchemeduc
Peer Reviewed: Y
Page Count: 6
Publication Date: 2014
Sponsoring Agency: US Department of Energy
Contract Number: DE-AC04-94AL85000
Document Type: Journal Articles
Reports - Descriptive
Descriptors: Science Education, Science Experiments, Scientific Research, Interdisciplinary Approach, Laboratory Experiments, Scientific Methodology, Spectroscopy, Synthesis, Physical Sciences, Chemistry, Radiation, Science Process Skills, Teaching Methods, Science Activities, Hands on Science, Films
DOI: 10.1021/ed500238j
ISSN: 0021-9584
Abstract: Introducing students to a multidisciplinary research laboratory presents challenges in terms of learning specific technical skills and concepts but also with respect to integrating different technical elements to form a coherent picture of the research. Here we present a multidisciplinary series of experiments we have developed in the Electronic, Optical, and Nano Materials group at Sandia National Laboratories to introduce students to essential experimental methods and concepts spanning thin film synthesis, crystallography, electrochemistry, and optical spectroscopy. With minimal assistance from a qualified instructor, students apply a sol-gel method to synthesize electrochromic tungsten oxide (WO[subscript3]) thin films and evaluate their performance with electrochemistry, UV-vis spectroscopy, and X-ray diffraction. We find that the color changing WO[subscript3] films capture the students' attention, are technologically relevant, and make excellent materials platforms for multidisciplinary research as they invite investigation with a range of laboratory techniques. The variety of experimental methods combined here challenges the students to correlate the interplay between structure, processing, and properties central to materials science. The modular nature of this experiment set permits it to be tailored to the time constraints of individual students and also allows it to be applied to upper-level materials science or chemistry laboratories.
Abstractor: As Provided
Number of References: 30
Entry Date: 2014
Accession Number: EJ1048323
Database: ERIC
Description
Abstract:Introducing students to a multidisciplinary research laboratory presents challenges in terms of learning specific technical skills and concepts but also with respect to integrating different technical elements to form a coherent picture of the research. Here we present a multidisciplinary series of experiments we have developed in the Electronic, Optical, and Nano Materials group at Sandia National Laboratories to introduce students to essential experimental methods and concepts spanning thin film synthesis, crystallography, electrochemistry, and optical spectroscopy. With minimal assistance from a qualified instructor, students apply a sol-gel method to synthesize electrochromic tungsten oxide (WO[subscript3]) thin films and evaluate their performance with electrochemistry, UV-vis spectroscopy, and X-ray diffraction. We find that the color changing WO[subscript3] films capture the students' attention, are technologically relevant, and make excellent materials platforms for multidisciplinary research as they invite investigation with a range of laboratory techniques. The variety of experimental methods combined here challenges the students to correlate the interplay between structure, processing, and properties central to materials science. The modular nature of this experiment set permits it to be tailored to the time constraints of individual students and also allows it to be applied to upper-level materials science or chemistry laboratories.
ISSN:0021-9584
DOI:10.1021/ed500238j